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:: Volume 4, Issue 68 (10-2018) ::
JMP 2018, 4(68): 122-135 Back to browse issues page
Comparison of Head Space Solid Phase Microextraction (HS-SPME) and Hydro-distillation (HD) Techniques in Determination of Essential Oils in Fritillaria imperialis
SS Seyed Saleh 1, S Arabi * 2, F Ashouri 1
1- Department on Essential Oils Technology, Pharmaceutical Sciences Branch, Islamic Azad University, Tehran, Iran
2- Department of Chemistry, Safadasht Branch, Islamic Azad University, Tehran, Iran , siminarabi1354@yahoo.com
Abstract:   (208 Views)
Background: Fritillaria imperialis is an endangered species with pharmaceutical alkaloids that can be effective in reducing blood pressure and reducing cardiac palpitations.  
Objective: Comparison of head space solid phase microextraction (HS-SPME) and hydro-distillation (HD) techniques in determination of essential oils in Fritillaria imperialis
Methods: Quality and quantity determination of components of extracted essential oils from aerial parts of Fritillaria imperialis by Head space-Solid phase microextraction (HS-SPME) and hydro-distillation (HD) techniques using Gas Chromatography-Mass Spctroscopy (GC-MS) method.
Results: 24 components (86.61%) were identified in the oil was isolated by hydrodistillation. The major components of oil of F.imperialis were α-Bisabolol oxide A (28.2%), Camphor (12.86%), Chamazulene (11.8%), Trans-Thujone (10.9%), α-Bisabolone oxide A (10.3%), δ-3-Carene (6.9%) and α-Pinene (5.65%). 21 components (94.93%) were characterized in the oil which was obtained by Head space-solid phase microextraction (HS-SPME). The major components of the oil were α-Bisabolol oxide A (35.2%), Camphor (9.54%), Chamazulene (18.3%), Trans-Thujone (7.89%), α-Bisabolone oxide A (11.8%), δ-3-Carene (6.5%) and α-Pinene (5.7%).  
Conclusion: In both methods (HD & HS-SPME), oxygenated sesquiterpenes were the main components of the oil, whereas hydrocarbon sesquiterpens were trace.
Keywords: Fritillaria imperialis, GC-MS, Head space solid phase microextraction (HS-SPME), Hydrodistillation (HD)
Full-Text [PDF 542 kb]   (78 Downloads)    
Type of Study: Research | Subject: Chemistry
Received: 2018/09/29 | Accepted: 2018/09/29 | Published: 2018/09/29
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Seyed Saleh S, Arabi S, Ashouri F. Comparison of Head Space Solid Phase Microextraction (HS-SPME) and Hydro-distillation (HD) Techniques in Determination of Essential Oils in Fritillaria imperialis. JMP. 2018; 4 (68) :122-135
URL: http://jmp.ir/article-1-2298-en.html


Volume 4, Issue 68 (10-2018) Back to browse issues page
فصلنامه علمی پژوهشی گیاهان دارویی Journal of Medicinal Plants
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